反应条件
1: 86 percent / 1.) n-BuLi, 2.) Li / 1.) THF-hexane, 0 deg C, 2.) NH3 liq.m, -70 deg C, 5 min 2: 75 percent / 1.) n-BuLi / 1.) THF-hexane, -45 deg C, 40 min, 2.) -45 deg C, 40 min; -> 10 deg C 1 h 3: Li / diethyl ether; liquid ammonia / -65 °C / other reagent, solvent, temperature View Scheme
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 32, p. 1412 - 1417
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 7 p. 1562 - 1568
