反应条件
in neat (no solvent)
Rh acetate was refluxed in soln. of butyric acid and butyric anhydride at 100°C (P=150 mmHg) for 3 h under N2; solvent was distilled off, cooled at -20°C overnight, filtered, rinsed with cold pentane, solid extd. with hot benzene, filtered, filtrate was concd., filtered, rinsed with cold pentane, dried in vac. for several h at 100°C; elem. anal.;
参考文献
Drago, Russell S.; Long, John R.; Cosmano, Richard
Inorganic Chemistry, 1981 , vol. 20, p. 2920 - 2927
