tributyl-amine; PdCl2*4P(o-Tol)3; potassium carbonate in water
T=100°C; 6 h;
参考文献
Bumagin, N. A.; Sukhomlinova, L. I.; Tolstaya, T. P.; Beletskaya, I. P.
Doklady Chemistry, 1993 , vol. 332, # 4 p. 221 - 224
Dokl. Akad. Nauk SSSR Ser. Khim., 1993 , vol. 332, # 4 p. 454 - 456
bis (triortho-tolylphosphine)palladium(II) chloride; tributyl-amine; potassium carbonate; tris-(o-tolyl)phosphine in water
T=100°C; 6 h;
参考文献
Bumagin, N. A.; Bykov, V. V.; Sukhomlinova, L. I.; Tolstaya, T. P.; Beletskaya, I. P.
Journal of Organometallic Chemistry, 1995 , vol. 486, # 1-2 p. 259 - 262
1.1: n-BuLi / tetrahydrofuran; hexane / 2 h / -60 °C
1.2: CeCl3 / tetrahydrofuran; hexane / 1 h / -60 °C
1.3: tetrahydrofuran; hexane / -60 - 20 °C
2.1: 0.14 g / p-TsOH / toluene / 12 h / Heating
View Scheme
参考文献
Klokkenburg, Mark; Lutz, Martin; Spek, Anthony L.; Van der Maas, John H.; Van Walree, Cornelis A.
Chemistry - A European Journal, 2003 , vol. 9, # 15 p. 3544 - 3554