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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
对溴甲苯
合成路线
（共 1677 条）
106-38-7
对溴甲苯
→
反应条件
4630-20-0
3-甲基咔唑
反应条件
1: 63.6 percent / K2CO3; Cu / nitrobenzene / 16 h / Heating 2: 71.5 percent / H2O; HCl / 0.5 h / Heating 3: 52.3 percent / Pd(OAc)2; AcOH / 1 h / Heating 4: Zn / 2 h / Heating View Scheme
参考文献
Chowdhury; Jha; Bhattacharyya; Mukherjee
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001 , vol. 40, # 6 p. 490 - 494
106-38-7
对溴甲苯
→
反应条件
486455-30-5
反应条件
1: 94 percent / aq. Na2CO3; Pd(PPh3)4 / ethanol; toluene / 1 h / Heating 2: 85 percent / aq. HI / 2 h / Heating View Scheme
参考文献
Nioche, J. Y.; Decerprit, J.; Festal, D.
European Journal of Medicinal Chemistry, 1995 , vol. 30, # 5 p. 377 - 386
106-38-7
对溴甲苯
+
214360-76-6
3-羟基苯硼酸频哪酯
→
反应条件
486455-30-5
反应条件
potassium carbonate in water; isopropyl alcohol Suzuki-Miyaura Coupling; 3 h; Green chemistry;
参考文献
Pandarus, Valerica; Gingras, Genevieve; Beland, Francois; Ciriminna, Rosaria; Pagliaro, Mario
Beilstein Journal of Organic Chemistry, 2014 , vol. 10, p. 897 - 901
106-38-7
对溴甲苯
→
反应条件
4926-78-7
顺式-1-乙基-4-甲基环己烷
反应条件
1: sodium; dipropyl ether 2: platinum / 175 °C / Hydrogenation View Scheme
参考文献
Kasanskii; Liberman
Doklady Akademii Nauk SSSR, 1955 , vol. 101, p. 877,879
Chem.Abstr., 1956 , p. 3254
106-38-7
对溴甲苯
+
100-39-0
溴化苄
→
反应条件
5023-60-9
反应条件
palladium diacetate; potassium carbonate; thiourea; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in water T=20°C; 4 h; Inert atmosphere;
参考文献
Wang, Liang; Zhou, Wei-You; Chen, Sheng-Chun; He, Ming-Yang; Chen, Qun
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 5 p. 839 - 845
106-38-7
对溴甲苯
+
100-53-8
苄硫醇
→
反应条件
5023-60-9
反应条件
1: phenylmethanethiol With sodium t-butanolate in tetrahydrofuran T=23°C; 0.166667 h; Inert atmosphere; 2: With zinc(II) chloride in tetrahydrofuran 0.166667 h; Inert atmosphere; 3: para-bromotoluene With [P(t-Bu)3Pd(μ-Br)]2; lithium iodide in tetrahydrofuran T=90°C; 2 h; Inert atmosphere;
参考文献
Bastug, Gulluzar; Nolan, Steven P.
Journal of Organic Chemistry, 2013 , vol. 78, # 18 p. 9303 - 9308
451-40-1
二苯基乙酮
+
106-38-7
对溴甲苯
→
反应条件
50353-99-6
反应条件
caesium carbonate; bis(phosphinite) PCR-pincer palladacycle; tetraphenyl deriv in N,N-dimethyl-formamide T=153°C; 1 h;
参考文献
Churruca, Fatima; SanMartin, Raul; Tellitu, Imanol; Dominguez, Esther
Tetrahedron Letters, 2006 , vol. 47, # 19 p. 3233 - 3237
106-38-7
对溴甲苯
+
15784-52-8
→
反应条件
50390-51-7
2,4'-二甲基苯丙酮
反应条件
1: With 1,1'-bis-(diphenylphosphino)ferrocene; 1,10-phenanthroline; Pd(F6-acac)2; cyclohexylamine; copper(I) bromide in quinoline T=100°C; 36 h; Inert atmosphereMolecular sieve; 2: With hydrogenchloride in tetrahydrofuran; quinoline; water T=80°C; 1 h; Inert atmosphere;
参考文献
Collet, Florence; Song, Bingrui; Rudolphi, Felix; Goossen, Lukas J.
European Journal of Organic Chemistry, 2011 , # 32 p. 6486 - 6501
106-38-7
对溴甲苯
+
15784-52-8
+
108-91-8
环己胺
→
反应条件
50390-51-7
2,4'-二甲基苯丙酮
+
1358762-28-3
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; 1,10-phenanthroline; Pd(F6-acac)2; magnesium trifluoromethane sulfonate; copper(I) bromide in 1-methyl-pyrrolidin-2-one T=100°C; 16 h; Inert atmosphereMolecular sieve;
参考文献
Collet, Florence; Song, Bingrui; Rudolphi, Felix; Goossen, Lukas J.
European Journal of Organic Chemistry, 2011 , # 32 p. 6486 - 6501
106-38-7
对溴甲苯
→
反应条件
50446-43-0
4,4-二甲基-5-(对甲苯)-1,1:3,1-ter苯基
+
1279694-54-0
反应条件
2: 18-crown-6 ether; potassium hydroxide / benzene 3: SO3*dioxane / 1,4-dioxane; chloroform / 4.5 h / Reflux View Scheme
参考文献
Gaitzsch, Jens; Rogachev, Victor; Metz, Peter; Filimonov, Victor D.; Zahel, Martin; Kataeva, Olga
Journal of Sulfur Chemistry, 2011 , vol. 32, # 1 p. 3 - 16
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