1: With chloro-trimethyl-silane; magnesium in tetrahydrofuran T=-5 - 20°C; 0.5 h; 2: With hydrogen bromide in tetrahydrofuran; water Product distribution / selectivity;
1: With chloro-trimethyl-silane; magnesium in tetrahydrofuran T=-5 - 20°C; 0.5 h; 2: With hydrogen bromide in tetrahydrofuran; water Product distribution / selectivity;
1: With tri-tert-butyl phosphine; tetra-n-butylammonium difluorotriphenylsilicate(IV); bis(dibenzylideneacetone)-palladium(0) in toluene T=95°C; Inert atmosphere; 2: With silica gel in toluene
参考文献
Guo, Yong; Tao, Guo-Hong; Blumenfeld, Alex; Shreeve, Jean'ne M.
Organometallics, 2010 , vol. 29, # 7 p. 1818 - 1823
1: With tri-tert-butyl phosphine; tetra-n-butylammonium difluorotriphenylsilicate(IV); bis(dibenzylideneacetone)-palladium(0) in toluene T=95°C; Inert atmosphere; 2: With silica gel in toluene
参考文献
Guo, Yong; Tao, Guo-Hong; Blumenfeld, Alex; Shreeve, Jean'ne M.
Organometallics, 2010 , vol. 29, # 7 p. 1818 - 1823
Almansa, Carmen; Gomez, Luis A.; Cavalcanti, Fernando L.; De Arriba, Alberto F.; Rodriguez, Ricardo; Carceller, Elena; Garcia-Rafanell, Julian; Forn, Javier
Journal of Medicinal Chemistry, 1996 , vol. 39, # 11 p. 2197 - 2206
