反应条件
1: 1.) Mg / 1.) Et2O, reflux, 0.5 h; 2.) Et2O, -72 deg C, 2 h --> -20 deg C, 40 min 2: 1.) 70percent sodium bis(2-methoxyethoxy)aluminum hydride; 2.) 5percent HCl/MeOH / 1.) Et2O, 0 deg C, 1 h --> r.t., 0.5 h View Scheme
参考文献
Mori, Shigehiro; Aoyama, Toyohiko; Shioiri, Takayuki
Chemical & Pharmaceutical Bulletin, 1986 , vol. 34, # 4 p. 1524 - 1530
