calcium hydroxide powder; dicobalt octacarbonyl; methyl iodide in water; N,N-dimethyl-formamide 20 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 52, # 12 p. 2623 - 2625
calcium hydroxide powder; dicobalt octacarbonyl in water; N,N-dimethyl-formamide 20 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 52, # 12 p. 2623 - 2625
1: 1-chloro-4-bromobenzene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; 2: chloroformic acid ethyl ester in tetrahydrofuran; hexane T=-78°C; 3 h; 3: With ammonium chloride in tetrahydrofuran; hexane; water
Bodroux
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1903 , vol. 137, p. 711
Bulletin de la Societe Chimique de France, 1904 , vol. <3> 31, p. 29