反应条件
1: 4-bromo-phenol With di-isopropyl azodicarboxylate; triphenylphosphine; Wang resin in tetrahydrofuran T=20°C; 2: 4-ethylbenzeneboronic acid With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in ethylene glycol dimethyl ether; water T=80°C; Suzuki reaction; 3: With trifluoroacetic acid in dichloromethane 0.166667 h;
参考文献
Edsall Jr., Richard J; Harris, Heather A; Manas, Eric S; Mewshaw, Richard E
Bioorganic and medicinal chemistry, 2003 , vol. 11, # 16 p. 3457 - 3474