您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-溴苯酚
合成路线
（共 1087 条）
106-41-2
4-溴苯酚
→
反应条件
6842-78-0
4-丁氧基联苯
反应条件
1: potassium carbonate / acetone 2: 87 percent / sodium carbonate / tetrakis(triphenylphosphine)palladium / tetrahydrofuran; H2O / 30 h / 80 °C View Scheme
参考文献
Zeng, Qi; Li, Zhen; Dong, Yongqiang; Di, Chong'an; Qin, Anjun; Hong, Yuning; Ji, Li; Zhu, Zhichao; Jim, Cathy K. W.; Yu, Gui; Li, Qianqian; Li, Zhongan; Liu, Yunqi; Qin, Jingui; Tang, Ben Zhong
Chemical Communications, 2007 , # 1 p. 70 - 72
106-41-2
4-溴苯酚
+
124-63-0
甲烷磺酰氯
→
反应条件
68574-35-6
4-溴苯基甲烷磺酸酯
反应条件
pyridine 1.) 0 deg C, 15 min, 2.) 5 deg C, overnight;
参考文献
Olszewski; Marshalla; Sabat; Sundberg
Journal of Organic Chemistry, 1994 , vol. 59, # 15 p. 4285 - 4296
106-41-2
4-溴苯酚
+
1666-13-3
二苯基二硒醚
→
反应条件
80448-02-8
反应条件
[2,2']bipyridinyl; copper(l) iodide; magnesium in N,N-dimethyl-formamide T=200°C; 7 h; microwave irradiation;
参考文献
Kumar, Sangit; Engman, Lars
Journal of Organic Chemistry, 2006 , vol. 71, # 14 p. 5400 - 5403
106-41-2
4-溴苯酚
→
反应条件
809285-98-1
反应条件
1.1: potassium carbonate; potassium iodide / acetone / 48 h / Reflux 2.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere 2.2: trialkyl borate / -78 - 20 °C / Inert atmosphere 2.3: Inert atmosphere 3.1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol; toluene / 5 h / 80 °C / Inert atmosphere View Scheme
参考文献
Chen, Wei-Hong; Chang, Yi-Ting; Lee, Jey-Jau; Chuang, Wei-Tsung; Lin, Hong-Cheu
Chemistry - A European Journal, 2011 , vol. 17, # 47 p. 13182 - 13187
106-41-2
4-溴苯酚
→
反应条件
81147-94-6
4-(环氧乙烷甲氧基)-苯丙酸甲酯
反应条件
1.1: palladium (II) trifluoroacetate; 2,2,2-trimethylacetic acid; potassium carbonate / 120 °C / |Schlenk technique; |Inert atmosphere; |Sealed tube 2.1: sulfuric acid / 10 h / |Reflux; |Inert atmosphere; |Schlenk technique; |Sealed tube 3.1: potassium carbonate / acetone / 5 h / 20 °C / |Inert atmosphere; |Schlenk technique; |Sealed tube 3.2: 20 h / |Reflux; |Schlenk technique; |Inert atmosphere; |Sealed tube View Scheme
参考文献
Wei, Yu; Tang, Huarong; Cong, Xuefeng; Rao, Bin; Wu, Chao; Zeng, Xiaoming
Organic Letters, 2014 , vol. 16, # 8 p. 2248 - 2251
106-41-2
4-溴苯酚
+
115-19-5
2-甲基-3-丁炔-2-醇
→
反应条件
82305-04-2
6-溴-2,2-二甲基-2H-苯并吡喃
反应条件
boron trifluoride diethyl etherate in dichloromethane T=20°C; 6.5 h;
参考文献
Madabhushi, Sridhar; Jillella, Raveendra; Godala, Kondal Reddy; Mallu, Kishore Kumar Reddy; Beeram, China Ramanaiah; Chinthala, Narsaiah
Tetrahedron Letters, 2012 , vol. 53, # 39 p. 5275 - 5279
106-41-2
4-溴苯酚
+
107-86-8
3-甲基-2-丁烯醛
→
反应条件
82305-04-2
6-溴-2,2-二甲基-2H-苯并吡喃
反应条件
acetic acid; 3,4,5-trimethoxyphenylboronic acid in toluene 16 h; Heating;
参考文献
Chauder, Brian A.; Lopes, Claudio C.; Lopes, Rosangela S. C.; Da Silva, Alcides J. M.; Snieckus, Victor
Synthesis, 1998 , # 3 p. 279 - 282
106-41-2
4-溴苯酚
→
反应条件
82305-04-2
6-溴-2,2-二甲基-2H-苯并吡喃
反应条件
1: potassium carbonate; sodium iodide / acetone / 72 h / 70 °C / |Inert atmosphere 2: N,N-dimethyl-aniline / 4 h / 200 °C / |Inert atmosphere View Scheme
参考文献
Dai, Wen; Li, Jun; Li, Guosong; Yang, Hua; Wang, Lianyue; Gao, Shuang
Organic Letters, 2013 , vol. 15, # 16 p. 4138 - 4141
106-41-2
4-溴苯酚
→
反应条件
82413-21-6
(E)-4’-羟基他莫昔芬
反应条件
1: 85 percent / NaH, DMF / 3 h / 85 - 90 °C 2: 1.) C2H5MgBr, 3.) HCl View Scheme
参考文献
Ruenitz, Peter C.; Bagley, Jerome R.; Mokler, Corwin M.
Journal of Medicinal Chemistry, 1982 , vol. 25, # 9 p. 1056 - 1060
622-40-2
2-吗啉乙醇
+
106-41-2
4-溴苯酚
→
反应条件
836-59-9
4-[2-(4-溴苯氧基)乙基]吗啉
反应条件
di-isopropyl azodicarboxylate; triphenylphosphine in tetrahydrofuran T=110°C; Mitsunobu Displacement; 17 h; Inert atmosphere;
参考文献
PFIZER INC.; Bhattacharya, Samit; Cameron, Kimberly; Dowling, Matthew; Fernando, Dilinie; Ebner, David; Filipski, Kevin; Kung, Daniel; Lee, Esther; Smith, Aaron; Tu, Meihua
Patent: US2013/267493 A1, 2013 ;
Location in patent: Paragraph 0804 ;
首页
上一页
1
...
91
92
93
94
95
96
97
...
109
下一页
末页
到第
页
确定
