Nassif, Larissa; Jakli, Antal; Seed, Alexander J.
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2001 , vol. 365, p. 171 - 179
1.1: 82 percent / imidazole / CH2Cl2 / 12.5 h / 0 - 20 °C
2.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C
2.2: triisopropyl borate / tetrahydrofuran; hexane / 5 h / -78 - 20 °C
2.3: 68 percent / aq. HCl / tetrahydrofuran; hexane / 0.5 h / 0 °C
3.1: 36 percent / Cu(OAc)2; Et3N; pyridine / 4 Angstroem molecular sieves / CH2Cl2 / 20 °C
View Scheme
参考文献
Hart, Matthew E.; Suchland, Katherine L.; Miyakawa, Motonori; Bunzow, James R.; Grandy, David K.; Scanlan, Thomas S.
Journal of Medicinal Chemistry, 2006 , vol. 49, # 3 p. 1101 - 1112
Zhang, Jiadi; Bellomo, Ana; Creamer, Andrea D.; Dreher, Spencer D.; Walsh, Patrick J.
Journal of the American Chemical Society, 2012 , vol. 134, # 33 p. 13765 - 13772