1: poly(phenylmethylsiloxane) With potassium carbonate in toluene T=20°C; 1 h; 2: 4-methyl-chlorobenzene With [(P{(C6H11)3})2Pd(Cl)2] in toluene T=120°C;
Cs2CO3; diiodobis(1,3-di[(R)-1-phenylethyl]imidazolin-2-ylidene)palladium(II) in xylene the mixt. in xylene was heated at 130°C (N2); H2O was added, the aq. phase was extd. with diethyl ether, the organic phase was dried over MgSO4;
参考文献
Herrmann, Wolfgang A.; Boehm, Volker P.W.; Gstoettmayr, Christian W.K.; Grosche, Manja; Reisinger, Claus-Peter; Weskamp, Thomas
Journal of Organometallic Chemistry, 2001 , vol. 617-618, p. 616 - 628