反应条件
Multi-step reaction with 2 steps 1.1: 4-(N,N-dimethlyamino)pyridine / dichloromethane / 0 - 20 °C / |Inert atmosphere2.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / |Inert atmosphere2.2: 0 - 20 °C / |Inert atmosphere
参考文献
Zhu, Manghong; Zhang, Chen; Nwachukwu, Jerome C.; Srinivasan, Sathish; Cavett, Valerie; Zheng, Yangfan; Carlson, Kathryn E.; Dong, Chune; Katzenellenbogen, John A.; Nettles, Kendall W.; Zhou, Hai-Bing Organic and Biomolecular Chemistry, 2012 , vol. 10, # 43 p. 8692 - 8700