1: With fluorspar; sulfuric acid; sodium nitrite in dichloromethane T=0°C; Diazotization; 0.25 h; 2: With water in dichloromethane T=55°C; Substitution; fluoro de-diazonization; 2 h; Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 11 p. 1491 - 1494
1: With sodium hydride in tetrahydrofuran; mineral oil T=20°C; 1 h; Inert atmosphere; 2: With naphthalene; sodium in tetrahydrofuran; mineral oil T=20°C; 12 h; Inert atmosphere; 3: With water in tetrahydrofuran; mineral oil Inert atmosphere;
