1: 2-methyl-propan-2-ol; H2O / 3 h / 20 - 25 °C / Irradiation; DRL-400 mercury lamp (400 W) 2: KOH / H2O / 0.33 h / Heating 3: air / H2O / 3 h / Ambient temperature View Scheme
参考文献
Frolov, A. N.; Klokova, E. M.; El'tsov, A. V.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, p. 1926 - 1935
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 10 p. 2161 - 2170
1: 1.) NaH (60percent in oil) / 1.) DMSO, 2.) DMSO, 85 deg C, 24 h 2: 62 percent / SnCl2*2H2O, conc. HCl / acetic acid / 3 h / Heating View Scheme
参考文献
Sjogren, Eric B.; Rider, Michael A.; Nelson, Peter H.; Bingham, Stanford; Poulton, Anthony L.; et al.
Journal of Medicinal Chemistry, 1991 , vol. 34, # 11 p. 3295 - 3301