1: Diazotization.Kochen der Diazoniumbromidloesung mit einer bromwasserstoffsauren Loesung von KBr und CuBr 2: sodium; diethyl ether 3: nitric acid / 150 - 160 °C / im geschlossenen Rohr View Scheme
参考文献
Acree
Chemische Berichte, 1904 , vol. 37, p. 993
American Chemical Journal, 1905 , vol. 33, p. 194
1: 66 percent / benzene; pyridine / 3 h / Ambient temperature 2: 65 percent / P2S5 / benzene / 4 h / Heating 3: 55 percent / 15percent NaOH, K3Fe(CN)6 / H2O; ethanol / 4 h / 80 - 90 °C 4: 52 percent / 47percent HBr / 24 h / Heating 5: 85 percent / tetrahydrofuran / 0.25 h / 0 - 5 °C 6: Ag2O / H2O / 0.75 h / 5 - 10 °C 7: 6 percent / phenothiazine / H2O; benzene / 1 h / Heating View Scheme
参考文献
Mashraqui, Sabir H.; Biswas, Maloyesh M.; Nivalkar, Kishor R.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1996 , vol. 35, # 10 p. 1031 - 1037
