in tetrahydrofuran dropwise addn. of 2.0M BH3*THF (25 mmol) to a THF soln. of the amine (10 mmol); performed under a dry N2 atm.;; removal of solvent and excess of BH3*THF under reduced pressure immediately after addn.;;
参考文献
Camacho, C.; Paz-Sandoval, M. A.; Contreras, R.
Polyhedron, 1986 , vol. 5, p. 1723 - 1732
