反应条件
1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / -78 - 20 °C / |Inert atmosphere
1.2: 3.5 h / -78 - 20 °C / |Inert atmosphere
2.1: silver hexafluoroantimonate / dichloromethane / 0.67 h / -78 °C / |Inert atmosphere; |Schlenk technique
View Scheme
参考文献
Betterley, Nolan M.; Surawatanawong, Panida; Prabpai, Samran; Kongsaeree, Palangpon; Kuhakarn, Chutima; Pohmakotr, Manat; Reutrakul, Vichai
Organic Letters, 2013 , vol. 15, # 22 p. 5666 - 5669