1: 80.7 percent Turnov. / Ba(OH)2*8H2O / methanol; benzene / 20 h / Ambient temperature
2: 45 percent / lead tetraacetate, pyridine, Cu(OAc)2 / benzene / 3 h / Heating
3: 1) Br2, 2) aq.KOH / 1) CCl4, r.t., 2) 135-145 deg C, 4 h
4: 86.2 percent / conc.H2SO4 / 4 h / Heating
5: 96 percent / LAH / diethyl ether / 2 h / Ambient temperature
6: 90.6 percent / PPTS / CH2Cl2 / 4 h / Ambient temperature
View Scheme
参考文献
Ranganathan, S.; Maniktala, Vibha; Kumar, Raaj; Singh, G. P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 12 p. 1197 - 1207
Zakharkin,L.I.; Khorlina,I.M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1964 , # 3 p. 435 - 438
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1964 , # 3 p. 465 - 469