potassium carbonate in acetone 48 h; RefluxInert atmosphere;
参考文献
Chavez, Sherry A.; Martinko, Alexander J.; Lau, Corinna; Pham, Michael N.; Cheng, Kui; Bevan, Douglas E.; Mollnes, Tom E.; Yin, Hang
Journal of Medicinal Chemistry, 2011 , vol. 54, # 13 p. 4659 - 4669
1: With tin(IV) chloride T=60 - 70°C; 3 h; 2: With sodium hydroxide; water T=90°C; 3 h; 3: With hydrogenchloride in water Product distribution / selectivity;
参考文献
Daicel Chemical Industries, Ltd.
Patent: US2007/49775 A1, 2007 ;
Location in patent: Page/Page column 6 ;