in tetrahydrofuran addn. of vinyl bromide and ethylene dibromide to Mg in THF (N2 atmosphere), addn. of further vinyl bromide in THF during 1 h at reflux, decantation, addn. of Sn-compd., refluxing (1 h), cooling room temp.); chromy. (Chromosorb G, 185°C); elem. anal.;
参考文献
Moloney, Mark G.; Pinhey, John T.; Stoermer, Martin J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry, 1990 , p. 2645 - 2656
Schouten
Recueil des Travaux Chimiques des Pays-Bas, 1937 , vol. 56, p. 541,554, 863, 871
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Schouten
Recueil des Travaux Chimiques des Pays-Bas, 1937 , vol. 56, p. 557,872
