tetrabutylammomium bromide; potassium carbonate in water; benzene 6 h; Heating;
参考文献
Puntambekar, Hemalata M; Naik, D G; Kapadi, A H
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1993 , vol. 32, # 7 p. 793 - 794
in not given other Radiation; formation at reaction of Sn-powder and 1-bromo-propane with (60)Co-γ-radiation;;
参考文献
Gmelin Handbook: Sn: MVol.C1, 7.7.1.2, page 387 - 387
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Wyant, R. E.; McFarling, J. L.; Kirchner, J. F.; Kahler, E. J.
BMI-1654 (1963) 1/12
n-butyllithium 1.) THF, -5-(-10) grad C, 30 min, nitrogen, 2.) THF, 1 h at -5-(-10) grad C then 24 h at room temp.; Yield given. Multistep reaction. Yields of byproduct given;
