diethyl ether; magnesium anschliessend mit Kohlendioxid;
参考文献
Wotiz et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 5503
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Gaudemar
Annales de Chimie (Cachan, France), 1956 , vol. <13>1, p. 161,184,186
1: BPB hydrochloride With Ni(NO3)2·6H2O; sodium hydride; glycine; potassium hydroxide in methanol T=50°C; 2 h; Inert atmosphereReflux; 2: propargyl bromide With tetra-(n-butyl)ammonium iodide; sodium hydroxide in dichloromethane; water T=20°C; 1 h; 3: With hydrogenchloride in methanol; water 2 h; Reflux;
参考文献
Lee, Dong Jun; Mandai, Kalyaneswar; Harris, Paul W. R.; Brimble, Margaret A.; Kent, Stephen B. H.
Organic Letters, 2009 , vol. 11, # 22 p. 5270 - 5273
