反应条件
1: (tosyl)NH(tert-butoxycarbonyl) With potassium carbonate in N,N-dimethyl-formamide
T=20°C; 1 h;
2: propargyl bromide in N,N-dimethyl-formamide
T=20°C; 2 h;
3: With trifluoroacetic acid in dichloromethane
T=20°C;
参考文献
Benedetti, Erica; Simonneau, Antoine; Hours, Alexandra; Amouri, Hani; Penoni, Andrea; Palmisano, Giovanni; Malacria, Max; Goddard, Jean-Philippe; Fensterbank, Louis
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 1908 - 1912