in deuterated toluene
Kinetics; degassing soln. of Cp*2ScCH2CHDPh in toluene-d8 (-78°C, NMR tube), condensing 2-butyne (-196°C), standing (room temp., 5 min); detected by 1H NMR;
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Shell Devel.Co.
Patent: US2803597 , 1949 ;