3,3-二乙氧基丙酸乙酯合成路线 (共 81 条)
反应条件
cerium(III) chloride; acetic acid in tert-butyl alcohol T=90°C; 6 h;
参考文献
Tamaso, Ken-Ichi; Hatamoto, Yuji; Sakaguchi, Satoshi; Obora, Yasushi; Ishii, Yasutaka
Journal of Organic Chemistry, 2007 , vol. 72, # 9 p. 3603 - 3605
反应条件
gadolinium(III) chloride hexahydrate in ethanol; acetic acid T=90°C; 6 h;
参考文献
Maeda, Sayuki; Obora, Yasushi; Ishii, Yasutaka
European Journal of Organic Chemistry, 2009 , # 24 p. 4067 - 4072
反应条件
sodium hydrogen sulphate Heating;
参考文献
Jacobsen, Niels; Winckelmann, Ib
Journal of Chemical Research, Miniprint, 1985 , # 3 p. 987 - 996
反应条件
1: aq. NH3 2: LiAlH4 / diethyl ether View Scheme
参考文献
Journal of medicinal chemistry, , vol. 16, # 1 p. 1 - 5
反应条件
sodium hydride in diethyl ether T=0 - 20°C; 15 h;
参考文献
EP1364946 A1, ;
Page/Page column 196 ;
参考文献
Tetrahedron Letters, , vol. 22, # 36 p. 3451 - 3454
反应条件
toluene-4-sulfonic acid T=100 - 110°C;
参考文献
Makin, S. M.; Kruglikova, R. I.; Kharitonova, O. V.; Arshava, B. M.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, p. 1846 - 1849
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 10 p. 2089 - 2093
反应条件
sodium hydrogen sulphate Heating;
参考文献
Jacobsen, Niels; Winckelmann, Ib
Journal of Chemical Research, Miniprint, 1985 , # 3 p. 987 - 996
反应条件
1: aqueous NH3 2: P2O5; triethylamine; benzene View Scheme
参考文献
McElvain; Clarke
Journal of the American Chemical Society, 1947 , vol. 69, p. 2660
反应条件
1: 85 percent / aq. NaOH / 0.5 h / 110 °C 2: SOCl2 / 1 h / 80 °C View Scheme
参考文献
Merial Limited; Meng, Charles Q.; Long, Alan; Huber, Scot; Gurrala, Srinivas Reddy; Wilkinson, Douglas Edward; Pacofsky, Gregory
Patent: US2014/142114 A1, 2014 ;