咪唑并[1,2-a]嘧啶-3-甲醛合成路线 (共 5 条)
反应条件
sodium hydroxide; trichlorophosphate in (2S)-N-methyl-1-phenylpropan-2-amine hydrate; N,N-dimethyl-formamide
参考文献
Merck and Co., Inc.
Patent: US4735956 A1, 1988 ;
US 4735956 A
反应条件
trichlorophosphate T=90°C; 5 h;
参考文献
Teulade, Jean C.; Bonnet, Pierre A.; Rieu, Jean N.; Viols, Henry; Chapat, Jean P.; et al.
Journal of Chemical Research, Miniprint, 1986 , # 6 p. 1842 - 1874
反应条件
calcium carbonate in water Heating;
参考文献
Chavignon; Teulade; Madesclaire; Gueiffier; Blache; Viols; Chapat; Dauphin
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 4 p. 691 - 697
反应条件
Tetra-n-butyl-ammonium 2-nitropropanate in water; toluene 24 h; Ambient temperatureIrradiation;
参考文献
Roubaud, Christine; Vanelle, Patrice; Maldonado, Jose; Crozet, Michel P.
Tetrahedron, 1995 , vol. 51, # 35 p. 9643 - 9656
反应条件
tetrabutylammomium bromide; lithium 1.) ethanol, 2.) toluene, water, RT, irradiation, 24 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Roubaud, Christine; Vanelle, Patrice; Maldonado, Jose; Crozet, Michel P.
Tetrahedron, 1995 , vol. 51, # 35 p. 9643 - 9656