2-(甲氧基甲基)苯甲醛合成路线 （共 10 条）
反应条件
pyridinium chlorochromate in dichloromethane 1.5 h; Ambient temperature;
参考文献
Kirmse, Wolfgang; Kund, Klaus
Journal of the American Chemical Society, 1989 , vol. 111, # 4 p. 1465 - 1473
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane; water 24 h; Ambient temperature;
参考文献
Wang, Wuyi; Li, Tiechao; Attardo, Giorgio
Journal of Organic Chemistry, 1997 , vol. 62, # 19 p. 6598 - 6602
反应条件
formic acid; nickel 36 h; Heating;
参考文献
Selassie, Cynthia Dias; Gan, Wei-Xi; Kallander, Lara S.; Klein, Teri E.
Journal of Medicinal Chemistry, 1998 , vol. 41, # 22 p. 4261 - 4272
反应条件
1.1: Na 2.1: DIBAL / benzene 2.2: HCl / H2O View Scheme
参考文献
Selassie, Cynthia Dias; Gan, Wei-Xi; Kallander, Lara S.; Klein, Teri E.
Journal of Medicinal Chemistry, 1998 , vol. 41, # 22 p. 4261 - 4272
反应条件
1: methanol / Ambient temperature 2: 53 percent / DDQ / CH2Cl2; H2O / 24 h / Ambient temperature View Scheme
参考文献
Wang, Wuyi; Li, Tiechao; Attardo, Giorgio
Journal of Organic Chemistry, 1997 , vol. 62, # 19 p. 6598 - 6602
反应条件
1.1: NaH / tetrahydrofuran 1.2: tetrahydrofuran 2.1: MnO2 / CHCl3 View Scheme
参考文献
Huebener, Gerd; Lambacher, Armin; Fromherz, Peter
Journal of Physical Chemistry B, 2003 , vol. 107, # 31 p. 7896 - 7902
反应条件
n-butyllithium 1.) Et2O, -78 deg C, 1.5 h 2.) -78 deg C -> 20 deg C; Yield given. Multistep reaction;
参考文献
Nakamura, Yosuke; O-kawa, Kyoji; Minami, Satoshi; Ogawa, Toshio; Tobita, Seiji; Nishimura, Jun
Journal of Organic Chemistry, 2002 , vol. 67, # 4 p. 1247 - 1252
反应条件
1: 87.5 percent / Na / 3 h / Heating 2: 1.) butyllithium / 1.) Et2O, -78 deg C, 1.5 h 2.) -78 deg C -> 20 deg C View Scheme
参考文献
Christenson, Beritte; Hallnemo, Gerd; Ullenius, Christina
Tetrahedron, 1991 , vol. 47, # 26 p. 4739 - 4752
反应条件
1: 91 percent / ethanol / 1.) 60 deg C, 3 h, 2.) room temp., 3 h, 3.) -20 deg C, overnight 2: 0.2 M NaOC2H5 / ethanol / 2 h / Ambient temperature; Irradiation View Scheme
参考文献
Journal of the American Chemical Society, , vol. 111, # 4 p. 1465 - 1473
反应条件
1: (3-N,N-di-n-butylamino)benzyltriphenylphosphonium chloride With sodium methylate in methanol
T=60°C; 3 h;
2: 2-[(methoxymethyl)methyl]benzaldehyde in methanol
Heating;
参考文献
Huebener, Gerd; Lambacher, Armin; Fromherz, Peter
Journal of Physical Chemistry B, 2003 , vol. 107, # 31 p. 7896 - 7902
