5-甲基-2,4'-联吡啶合成路线 （共 6 条）
反应条件
1: With potassium tert-butylate in tetrahydrofuran T=20°C; Michael reaction; 0.5 h; 2: With ammonium acetate; acetic acid T=95°C; 6 h;
参考文献
Kuwabara, Hirokazu; Umihara, Ken; Furugori, Yasushi; Itoh, Isamu
Chemistry Letters, 2005 , vol. 34, # 6 p. 834 - 835
反应条件
potassium hydroxide; tetrabutylammomium bromide; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran 3 h; Heating;
参考文献
Ishikura; Ohta; Terashima
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 11 p. 4755 - 4763
反应条件
1: With potassium tert-butylate in tetrahydrofuran T=40°C; Michael reaction; 0.166667 h; 2: With ammonium acetate; acetic acid T=90°C; 3 h;
参考文献
Kuwabara, Hirokazu; Umihara, Ken; Furugori, Yasushi; Itoh, Isamu
Chemistry Letters, 2005 , vol. 34, # 6 p. 834 - 835
反应条件
C14H25N2(1+)*BF4(1-); potassium tert-butylate; ammonium acetate; acetic acid
参考文献
Su, Shengqun; Chen, Wan; Song, Xuezhi; Zhu, Min; Qin, Chao; Song, Shuyan; Guo, Zhiyong; Wang, Song; Hao, Zhaoming; Li, Guanghua; Zhang, Hongjie
CrystEngComm, 2012 , vol. 14, # 5 p. 1681 - 1686
反应条件
potassium permanganate
参考文献
Su, Shengqun; Chen, Wan; Song, Xuezhi; Zhu, Min; Qin, Chao; Song, Shuyan; Guo, Zhiyong; Wang, Song; Hao, Zhaoming; Li, Guanghua; Zhang, Hongjie
CrystEngComm, 2012 , vol. 14, # 5 p. 1681 - 1686
反应条件
in isopropyl alcohol
T=50°C; 5 h;
参考文献
FUJIFILM FINECHEMICALS CO., LTD.
Patent: EP1657240 A1, 2006 ;
Location in patent: Page/Page column 33-34 ;
