4-甲基-2-丙炔-1,4-二醇合成路线 （共 16 条）
参考文献
Billington, David C.; Kerr, William J.; Pauson, Peter L.
Journal of Organometallic Chemistry, 1987 , vol. 328, p. 223 - 228
反应条件
1: propargyl alcohol With ethylmagnesium bromide in tetrahydrofuran; diethyl ether T=20°C; 3 h; 2: acetone in tetrahydrofuran; diethyl ether T=20°C;
参考文献
Mdachi
Bulletin of the Chemical Society of Ethiopia, 2012 , vol. 26, # 1 p. 103 - 113
反应条件
copper Hydroxide; calcium carbonate
参考文献
I.G.Farbenind.
Patent: DE728466 , 1938 ;
DRP/DRBP Org.Chem.
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Reppe,W.
Acetylene Chemistry <New York 1949>S.83
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Reppe et al.
Justus Liebigs Annalen der Chemie, 1955 , vol. 596, p. 65
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Gen.Aniline and Film Corp.
Patent: US2238471 , 1939 ;
参考文献
Vlasov,V.M. et al.
Journal of Organic Chemistry USSR (English Translation), 1967 , vol. 3, p. 261 - 263
Zhurnal Organicheskoi Khimii, 1967 , vol. 3, # 2 p. 277 - 280
反应条件
zuletzt bei Siedetemperatur; analoge Reaktionen mit Acetaldehyd unterhalb 0grad, mit 1-Methyl-cyclopentanon-(2) und mit Benzil in Aether bei 20grad;
参考文献
Nudenberg; Butz
Journal of the American Chemical Society, 1943 , vol. 65, p. 2059
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Newman; Fones; Booth
Journal of the American Chemical Society, 1945 , vol. 67, p. 1054
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Nasarow; Torgow
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 1336
Chem.Abstr., 1949 , p. 2161
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Salkind; Shurawlewa
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 984,987
Chem.Abstr., 1949 , p. 571
参考文献
I.G.Farbenind.
Patent: DE728466 , 1938 ;
DRP/DRBP Org.Chem.
反应条件
1: 93 percent / H2 / 10 percent Pd/C / ethyl acetate / 3 h / 20 °C 2: 88 percent / PDC / dimethylformamide / 3 h / 20 °C 3: 88 percent / DIBAL-H / CH2Cl2; toluene / 0.75 h / -20 °C View Scheme
参考文献
Martin, David Diez; Marcos, Isidro S.; Basabe, Pilar; Romero, Ricardo E.; Moro, Rosalina F.; Lumeras, Wenceslao; Rodriguez, Lucena; Urones, Julio G.
Synthesis, 2001 , # 7 p. 1013 - 1022
反应条件
1: 93 percent / H2 / 10 percent Pd/C / ethyl acetate / 3 h / 20 °C 2: 88 percent / PDC / dimethylformamide / 3 h / 20 °C View Scheme
参考文献
Martin, David Diez; Marcos, Isidro S.; Basabe, Pilar; Romero, Ricardo E.; Moro, Rosalina F.; Lumeras, Wenceslao; Rodriguez, Lucena; Urones, Julio G.
Synthesis, 2001 , # 7 p. 1013 - 1022
反应条件
1: Raney nickel / Hydrogenation 2: magnesium sulfate View Scheme
参考文献
Colonge et al.
Bulletin de la Societe Chimique de France, 1958 , p. 211,217
反应条件
1: Raney nickel / Hydrogenation 2: magnesium sulfate View Scheme
参考文献
Colonge et al.
Bulletin de la Societe Chimique de France, 1958 , p. 211,217
