N-Boc2-碘-4-氟苯胺合成路线 (共 2 条)
反应条件
1: 4-fluoroaniline With iodine; sodium hydrogencarbonate in water 2: di-tert-butyl dicarbonate With sodium hexamethyldisilazane in tetrahydrofuran
参考文献
Tetrahedron Letters, , vol. 53, # 29 p. 3742 - 3745
反应条件
1: caesium carbonate / acetonitrile / 20 °C 2: isopropylmagnesium chloride lithium chloride complex / tetrahydrofuran / 1 h / -78 °C 3: acetyl chloride / ethanol / 1.17 h / 20 - 50 °C View Scheme
参考文献
Kobayashi, Yuichi; Igarashi, Junji; Feng, Chao; Toshifumi; Tojo
Tetrahedron Letters, 2012 , vol. 53, # 29 p. 3742 - 3745