您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
106112-39-4
合成路线
（共 11 条）
106112-39-4
→
反应条件
106112-41-8
反应条件
1: 95 percent / copper / 4 h / 230 °C 2: 92 percent / N-bromosuccinimide / various solvent(s) / 6 h / 70 - 75 °C View Scheme
参考文献
Kajigaeshi, Shoji; Kadowaki, Toshiya; Nishida, Akiko; Fujisaki, Shizuo
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 97 - 104
106112-39-4
→
反应条件
58775-07-8
3,6-二叔丁基黄酮
反应条件
copper T=230°C; 4 h;
参考文献
Kajigaeshi, Shoji; Kadowaki, Toshiya; Nishida, Akiko; Fujisaki, Shizuo
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 97 - 104
106112-39-4
→
反应条件
7012-16-0
2,7-二氯芴
反应条件
1: 95 percent / copper / 4 h / 230 °C 2: 84 percent / iron, chlorine / CCl4 / 0.5 h / 30 °C 3: 37 percent / AlCl3 / benzene / 0.5 h / 50 °C View Scheme
参考文献
Kajigaeshi, Shoji; Kadowaki, Toshiya; Nishida, Akiko; Fujisaki, Shizuo
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 97 - 104
106112-39-4
→
反应条件
16433-88-8
2,7-二溴芴
反应条件
1: 95 percent / copper / 4 h / 230 °C 2: 92 percent / N-bromosuccinimide / various solvent(s) / 6 h / 70 - 75 °C 3: 43 percent / AlCl3 / benzene / 0.5 h / 50 °C View Scheme
参考文献
Kajigaeshi, Shoji; Kadowaki, Toshiya; Nishida, Akiko; Fujisaki, Shizuo
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 97 - 104
106112-39-4
→
反应条件
304-28-9
2,7-二(乙酰氨基)芴
反应条件
1: 95 percent / copper / 4 h / 230 °C 2: 45 percent / nitric acid, concd. sulfuric acid / acetic anhydride / 2 h / 15 - 20 °C 3: 98 percent / CaCl2, zinc / ethanol; H2O / 2 h / Heating 4: 93 percent / benzene / 0.33 h / 40 - 50 °C 5: 56 percent / AlCl3 / benzene / 0.5 h / 50 °C View Scheme
参考文献
Kajigaeshi, Shoji; Kadowaki, Toshiya; Nishida, Akiko; Fujisaki, Shizuo
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 97 - 104
106112-39-4
→
反应条件
58775-15-8
3,6-二叔丁基芴酮
反应条件
1: 85 percent / Zn / NiCl2(PPh3)2, PPh3 / dimethylformamide / 24 h / 70 - 75 °C 2: 80 percent / PDC, celite, t-BuOOH / benzene View Scheme
参考文献
Paul, Gitendra C.; Gajewski, Joseph J.
Organic Preparations and Procedures International, 1998 , vol. 30, # 2 p. 222 - 225
106112-39-4
→
反应条件
53535-88-9
反应条件
1: 82 percent / MeONa, CuI / dimethylformamide / 24 h / Heating 2: 11 percent / TiCl4 / CH2Cl2 / 3 h / Ambient temperature View Scheme
参考文献
Yamato, Takehiko; Sakaue, Naozumi; Shinoda, Naoki; Matsuo, Koji
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 8 p. 1193 - 1199
106112-39-4
→
反应条件
106112-42-9
反应条件
Multi-step reaction with 2 steps 1: 95 percent / copper / 4 h / 230 °C2: 84 percent / iron, chlorine / CCl4 / 0.5 h / 30 °C
参考文献
Kajigaeshi, Shoji; Kadowaki, Toshiya; Nishida, Akiko; Fujisaki, Shizuo Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 97 - 104
106112-39-4
→
反应条件
106112-43-0
反应条件
Multi-step reaction with 2 steps 1: 95 percent / copper / 4 h / 230 °C2: 45 percent / nitric acid, concd. sulfuric acid / acetic anhydride / 2 h / 15 - 20 °C
参考文献
Kajigaeshi, Shoji; Kadowaki, Toshiya; Nishida, Akiko; Fujisaki, Shizuo Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 97 - 104
106112-39-4
→
反应条件
106112-44-1
反应条件
Multi-step reaction with 3 steps 1: 95 percent / copper / 4 h / 230 °C2: 45 percent / nitric acid, concd. sulfuric acid / acetic anhydride / 2 h / 15 - 20 °C3: 98 percent / CaCl2, zinc / ethanol; H2O / 2 h / Heating
参考文献
Kajigaeshi, Shoji; Kadowaki, Toshiya; Nishida, Akiko; Fujisaki, Shizuo Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 97 - 104
1
2
下一页
末页
到第
页
确定
