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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
106112-41-8
合成路线
（共 7 条）
58775-07-8
3,6-二叔丁基黄酮
→
反应条件
106112-41-8
反应条件
N-bromosuccinmide in various solvent(s) T=70 - 75°C; 6 h;
参考文献
Kajigaeshi, Shoji; Kadowaki, Toshiya; Nishida, Akiko; Fujisaki, Shizuo
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 97 - 104
19099-48-0
4,4’-双叔丁基二苯基甲烷
→
反应条件
106112-41-8
反应条件
1: 54 percent / periodic acid, 98percent H2SO4 / H2O 2: 95 percent / copper / 4 h / 230 °C 3: 92 percent / N-bromosuccinimide / various solvent(s) / 6 h / 70 - 75 °C View Scheme
参考文献
Kajigaeshi, Shoji; Kadowaki, Toshiya; Nishida, Akiko; Fujisaki, Shizuo
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 97 - 104
58775-15-8
3,6-二叔丁基芴酮
→
反应条件
106112-41-8
反应条件
1: 93 percent / sodium borohydride / ethanol / 0.5 h / Heating 2: 90 percent / hydroiodic acid / acetic acid / 2 h / Heating 3: 92 percent / N-bromosuccinimide / various solvent(s) / 6 h / 70 - 75 °C View Scheme
参考文献
Kajigaeshi, Shoji; Kadowaki, Toshiya; Nishida, Akiko; Fujisaki, Shizuo
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 97 - 104
106112-40-7
→
反应条件
106112-41-8
反应条件
1: 90 percent / hydroiodic acid / acetic acid / 2 h / Heating 2: 92 percent / N-bromosuccinimide / various solvent(s) / 6 h / 70 - 75 °C View Scheme
参考文献
Kajigaeshi, Shoji; Kadowaki, Toshiya; Nishida, Akiko; Fujisaki, Shizuo
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 97 - 104
106112-39-4
→
反应条件
106112-41-8
反应条件
1: 95 percent / copper / 4 h / 230 °C 2: 92 percent / N-bromosuccinimide / various solvent(s) / 6 h / 70 - 75 °C View Scheme
参考文献
Kajigaeshi, Shoji; Kadowaki, Toshiya; Nishida, Akiko; Fujisaki, Shizuo
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 97 - 104
106112-41-8
→
反应条件
16433-88-8
2,7-二溴芴
反应条件
aluminium trichloride in benzene T=50°C; 0.5 h;
参考文献
Kajigaeshi, Shoji; Kadowaki, Toshiya; Nishida, Akiko; Fujisaki, Shizuo
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 97 - 104
106112-41-8
+
98-80-6
苯硼酸
→
反应条件
906097-52-7
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in ethanol; water; toluene 6 h; Heating / reflux;
参考文献
Fina Technology, Inc.
Patent: US8093418 B2, 2012 ;
Location in patent: Page/Page column 19 ;
