pyridine; 4-(N,N-dimethlyamino)pyridine in diethyl ether 0.333333 h; Ambient temperature;
参考文献
Barton, Derek H.R.; Crich, David; Kretzschmar, Gerhard
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 39 - 54
1: 90 percent / acetone / 4 h / Ambient temperature 2: 46 percent / anhydrous ZnCl2 / diethyl ether / 12 h / Ambient temperature 3: 92 percent / pyridine, DMAP / diethyl ether / 0.33 h / Ambient temperature View Scheme
参考文献
Barton, Derek H.R.; Crich, David; Kretzschmar, Gerhard
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 39 - 54
1: 46 percent / anhydrous ZnCl2 / diethyl ether / 12 h / Ambient temperature 2: 92 percent / pyridine, DMAP / diethyl ether / 0.33 h / Ambient temperature View Scheme
参考文献
Barton, Derek H.R.; Crich, David; Kretzschmar, Gerhard
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 39 - 54
1: NH2OH*HCl 2: 90 percent / acetone / 4 h / Ambient temperature 3: 46 percent / anhydrous ZnCl2 / diethyl ether / 12 h / Ambient temperature 4: 92 percent / pyridine, DMAP / diethyl ether / 0.33 h / Ambient temperature View Scheme
参考文献
Barton, Derek H.R.; Crich, David; Kretzschmar, Gerhard
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 39 - 54