2,4,6-三甲氧基-苯丙醛合成路线 (共 2 条)
反应条件
1: With phenyl silane; 4-methylmorpholine N-oxide; molybdenum hexacarbonate in tetrahydrofuran T=70°C; Inert atmosphere; 2: With water in tetrahydrofuran T=20°C; 0.208333 h; Inert atmosphere;
参考文献
Maki, Brooks E.; Scheldt, Karl A.
Organic Letters, 2008 , vol. 10, # 19 p. 4331 - 4334
反应条件
1: With sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene in water; tert-butyl alcohol
T=0 - 20°C; Pinnick oxidation; Inert atmosphere;
2: With ammonium chloride in water; tert-butyl alcohol
T=20°C; Inert atmosphere;
参考文献
Maki, Brooks E.; Chan, Audrey; Phillips, Eric M.; Scheidt, Karl A.
Tetrahedron, 2009 , vol. 65, # 16 p. 3102 - 3109