1,2,3,4-四氢异喹啉-1-羧酸乙酯合成路线 （共 11 条）
反应条件
hydrogen; acetic acid; Rh on carbon in ethanol
参考文献
Journal of Medicinal Chemistry, , vol. 29, # 10 p. 1953 - 1961
反应条件
1: molecular sieves 4 Angstroem / benzene / 25 °C 2: 55 percent / nBu3SnH; AIBN / benzene / 1 h / 85 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 125, # 1 p. 163 - 168
反应条件
1: 99 percent / H2 / Pt/C / acetic acid / 24 h / 25 °C / 45004.5 Torr 2: 54 percent / SOCl2 / 1 h / Heating View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 18, # 12 p. 1428 - 1433
反应条件
thionyl chloride 1 h; Heating;
参考文献
Paal, Tihamer A.; Forro, Eniko; Liljeblad, Arto; Kanerva, Liisa T.; Fueloep, Ferenc
Tetrahedron Asymmetry, 2007 , vol. 18, # 12 p. 1428 - 1433
反应条件
Yield given. Multistep reaction;
参考文献
Tetrahedron, , vol. 42, # 9 p. 2571 - 2574
反应条件
benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide in N,N-dimethyl-formamide Ambient temperature;
参考文献
Klutchko; Blankley; Fleming; Hinkley; Werner; Nordin; Holmes; Hoefle; Cohen; Essenburg
Journal of Medicinal Chemistry, 1986 , vol. 29, # 10 p. 1953 - 1961
反应条件
lipase B from Candida albicans; ammonium acetate in ethanol; water T=3°C; pH=8.0; 24 h; Enzymatic reaction;
参考文献
Paal, Tihamer A.; Liljeblad, Arto; Kanerva, Liisa T.; Forro, Eniko; Fueloep, Ferenc
European Journal of Organic Chemistry, 2008 , # 31 p. 5269 - 5276
反应条件
water; n-dipropylamine; lipase B from Candida antarctica in toluene; acetonitrile T=25°C; 192 h; Enzymatic reaction;
参考文献
Paal, Tihamer A.; Forro, Eniko; Liljeblad, Arto; Kanerva, Liisa T.; Fueloep, Ferenc
Tetrahedron Asymmetry, 2007 , vol. 18, # 12 p. 1428 - 1433
反应条件
water; lipase B from Candida antarctica in di-isopropyl ether T=3°C; 92 h; Enzymatic reaction;
参考文献
Paal, Tihamer A.; Forro, Eniko; Liljeblad, Arto; Kanerva, Liisa T.; Fueloep, Ferenc
Tetrahedron Asymmetry, 2007 , vol. 18, # 12 p. 1428 - 1433
反应条件
water; lipase B from Candida antarctica in di-isopropyl ether T=3°C; 92 h; Enzymatic reaction;
参考文献
Paal, Tihamer A.; Forro, Eniko; Liljeblad, Arto; Kanerva, Liisa T.; Fueloep, Ferenc
Tetrahedron Asymmetry, 2007 , vol. 18, # 12 p. 1428 - 1433
