反应条件
Multi-step reaction with 3 steps 1: 0.41 g / acetic acid / 26 h / 80 °C2: 1.) N-methylmorpholine N-oxide, osmium tetroxide; 2.) p-toluenesulfonic acid / 1.) t-butyl alcoho-THF-water (10.10:1), r.t., 18 h; 2.) CHCl3, r.t., 1 h3: trifluoroperacetic acid, Na2HPO4 (powdered) / CH2Cl2 / 1.) 5 deg C, 1 h; 2.) 30 deg C, 3 h
参考文献
Aburatani, Masakazu; Takeuchi, Tadashi; Mori, Kenji Agricultural and Biological Chemistry, 1987 , vol. 51, # 7 p. 1909 - 1914
