反应条件
in tetrahydrofuran Mixt. was stirred at room temp. over night;; H2O and ether was added to a soln., layers were sepd.; organic layer was washed with 20percent KF and brine, then dried over K2CO3, mixt. was dissolved in hot EtOH, filtered, crystd. by cooling, ppt. was chromd. on silica column (pentane); elem. anal.;;
参考文献
Organometallics, , vol. 6, p. 415 - 420
