反应条件
in tetrahydrofuran; diethyl ether under N2, addn. of a soln. of triphenylstannylmethyliodide in THF to a soln. of 2-lithiobenzothiazole in Et2O , stirring for 1 h at -78 ° C, warming up to room temp.; evapn., solving in cyclohexane/ethyl acetate 1/3, washing with water, organic layer dried over MgSO4, crystalline Ph3Sn2Ph3 obtained from petroleum ether;
参考文献
Journal of Organometallic Chemistry, , vol. 365, p. 61 - 74
