in further solvent(s) byproducts: mesitylene; absence of air and moisture; in C6D5Br; bubbling CO at 150°C for6 h; not isolated, reaction followed by (1)H-NMR spectroscopy;
参考文献
Journal of Organometallic Chemistry, , vol. 572, # 1 p. 11 - 20
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 36, p. 884 - 884
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 36, p. 956 - 957
in ethylene glycol dimethyl ether (vac.); to Ph3SnH was added soln. of Pr compd., react. was complete within 3-5 min at 20°C; ppt. was recrystd. from hexane, identified by m.p.;
参考文献
Journal of Organometallic Chemistry, , vol. 190, # 2 p. 157 - 166