Tsai, T. T.; Lehn, W. L.
Journal of Organic Chemistry, 1966 , vol. 31, p. 2981 - 2985
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Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.7.1, page 69 - 70
in tetrahydrofuran formation on reaction of ((C6H5)3Sn)2 and Li and decomposition with HCl;;
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Tamborski, C.; Ford, F. E.
Journal of Organic Chemistry, 1963 , vol. 28, p. 181 - 184
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Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.7.1, page 69 - 70
in tetrahydrofuran soln. of stannane addn. to soln. of YbI2 (in contact with Yb), reaction stopping with diluted HCl; reaction mixture extracting with ether, extracts drying (Na2SO4);
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Russian Journal of General Chemistry, , vol. 67, # 1 p. 76 - 78
in tetrahydrofuran soln. of RbYbI transferring dropwise under Ar pressure at room temperature, reaction mixture decomposing with 3percent HCl at 5°C; extracting with ether, extracts drying (Na2SO4);
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Russian Journal of General Chemistry, , vol. 67, # 1 p. 76 - 78
in tetrahydrofuran under Ar; addn. of freshly prepd. THF soln. of PhSmI to mixt. of THF and Ph3SnSnPh3, mixing at 25°C for 3 h, decompn. of react. mixt. with water acidified with HCl; thin layer chromy.;
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Russian Journal of General Chemistry, , vol. 70, # 2 p. 244 - 246
in tetrahydrofuran under Ar; addn. of freshly prepd. THF soln. of EtEuI contg. Eu/EuI2 ppt. to mixt. of THF and Ph3SnSnPh3, mixing at 25°C for 3 h, decompn. of react. mixt. with water acidified with HCl; thin layer chromy.;
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Russian Journal of General Chemistry, , vol. 70, # 2 p. 244 - 246
in tetrahydrofuran Ar atmosphere, RYbI transferring dropwise under Ar pressure at room temperature, 2 to 3 h, Ge-compd. addn.; extracting with ether, extracts drying (Na2SO4);
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Syutkina; Rybakova; Novgorodova; Petrov
Russian Journal of General Chemistry, 1997 , vol. 67, # 1 p. 76 - 78
in tetrahydrofuran Ar atmosphere, RYbI transferring dropwise under Ar pressure at room temperature, 2 to 3 h, Me3SnCl addn.; extracting with ether, extracts drying (Na2SO4);
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Syutkina; Rybakova; Novgorodova; Petrov
Russian Journal of General Chemistry, 1997 , vol. 67, # 1 p. 76 - 78
NiCl2((PPh3)P)2 in tetrahydrofuran
soln. of RbYbI transferring dropwise under Ar pressure at room temperature, CH3I addn. in presence of Ni-compd. (yield is only 5percent in absence of Ni-compd.);
参考文献
Syutkina; Rybakova; Novgorodova; Petrov
Russian Journal of General Chemistry, 1997 , vol. 67, # 1 p. 76 - 78
