5H-吡啶并[3,2:5,6]嘧啶并[2,1-b][1,3]噻唑-5-硫酮合成路线 （共 4 条）
反应条件
diphosphorus pentasulfide in pyridine 1 h; Heating;
参考文献
Monge; Martinez-Merino; Fernandex-Alvarez
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 2 p. 509 - 512
反应条件
1: pyridine / CHCl3 / 1 h / 70 °C 2: conc. HCl / dimethylformamide / 1 h / 120 °C 3: 85 percent / phosphorus pentasulfide / pyridine / 1 h / Heating View Scheme
参考文献
Monge; Martinez-Merino; Fernandex-Alvarez
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 2 p. 509 - 512
反应条件
1: thionyl chloride / 1.5 h / Heating 2: pyridine / CHCl3 / 1 h / 70 °C 3: conc. HCl / dimethylformamide / 1 h / 120 °C 4: 85 percent / phosphorus pentasulfide / pyridine / 1 h / Heating View Scheme
参考文献
Monge; Martinez-Merino; Fernandex-Alvarez
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 2 p. 509 - 512
反应条件
1: conc. HCl / dimethylformamide / 1 h / 120 °C 2: 85 percent / phosphorus pentasulfide / pyridine / 1 h / Heating View Scheme
参考文献
Monge; Martinez-Merino; Fernandex-Alvarez
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 2 p. 509 - 512
