呋喃并[2,3-c]吡啶-3(2H)-酮盐酸盐合成路线 （共 6 条）
反应条件
hydrogenchloride in water 6 h; Reflux;
参考文献
Array Biopharma, Inc.
Patent: US2010/63066 A1, 2010 ;
Location in patent: Page/Page column 30 ;
反应条件
1: 83 percent / 98percent H2SO4 / benzene / 48 h / Heating 2: 62 percent / K2CO3 anhydr. / acetone / 2 h / Heating 3: 74 percent / Na / toluene; ethanol / 6 h / Heating 4: 10percent HCl / 2.5 h / Heating View Scheme
参考文献
Morita, Hiroyuki; Shiotani, Shunsaku
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 549 - 552
反应条件
1: 74 percent / Na / toluene; ethanol / 6 h / Heating 2: 10percent HCl / 2.5 h / Heating View Scheme
参考文献
Morita, Hiroyuki; Shiotani, Shunsaku
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 549 - 552
反应条件
1: 62 percent / K2CO3 anhydr. / acetone / 2 h / Heating 2: 74 percent / Na / toluene; ethanol / 6 h / Heating 3: 10percent HCl / 2.5 h / Heating View Scheme
参考文献
Morita, Hiroyuki; Shiotani, Shunsaku
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 549 - 552
反应条件
sodium tetrahydroborate in methanol 0.5 h; Ambient temperature;
参考文献
Morita, Hiroyuki; Shiotani, Shunsaku
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 549 - 552
反应条件
1: 76 percent / sodium borohydride / methanol / 0.5 h / Ambient temperature 2: 82 percent / 85percent phosphoric acid / 18 h / 180 °C View Scheme
参考文献
Morita, Hiroyuki; Shiotani, Shunsaku
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 549 - 552
