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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
106536-15-6
合成路线
（共 8 条）
106536-15-6
→
反应条件
700-91-4
5-苯基-3,4-二氢-2H-吡咯
反应条件
1: tetrahydrofuran / 13 h / 0 - 20 °C 2: sodium iodide / acetone / 19 h / 20 °C / Inert atmosphere 3: water; lithium chloride / dimethyl sulfoxide / 3 h / 140 - 150 °C View Scheme
参考文献
More, Satish S.; Mohan, T. Krishna; Kumar, Y. Sateesh; Kumar, U.K. Syam; Patel, Navin B.
Beilstein Journal of Organic Chemistry, 2011 , vol. 7, p. 831 - 838
106536-15-6
→
反应条件
700-91-4
5-苯基-3,4-二氢-2H-吡咯
反应条件
1: tetrahydrofuran / 13 h / 0 - 20 °C 2: sodium iodide / acetone / 19 h / 20 °C / Inert atmosphere 3: water; lithium chloride / dimethyl sulfoxide / 12 h / 100 - 110 °C View Scheme
参考文献
More, Satish S.; Mohan, T. Krishna; Kumar, Y. Sateesh; Kumar, U.K. Syam; Patel, Navin B.
Beilstein Journal of Organic Chemistry, 2011 , vol. 7, p. 831 - 838
106536-15-6
→
反应条件
77037-46-8
反应条件
1: 70 percent / potassium carbonate / dimethylformamide / 12 h / 140 °C / Heating 2: 61 percent / polyphosphoric acid / 1 h / 100 °C / Heating View Scheme
参考文献
Hormi, Osmo E. O.; Moisio, M. Riitta; Sund, B. Christian
Journal of Organic Chemistry, 1987 , vol. 52, # 23 p. 5272 - 5274
106536-15-6
→
反应条件
50593-72-1
4-氯-6-甲氧基-2-苯基喹啉
反应条件
1: 78 percent / K2CO3 / dimethylformamide / 3 h / 140 °C 2: 82 percent / diphenyl ether / 1 h / 230 - 250 °C 3: 85 percent / NaOH / ethanol / 6 h / Heating 4: 92 percent / POCl3 / Heating View Scheme
参考文献
Zhao, Yue-Ling; Chen, Yeh-Long; Chang, Feng-Shuo; Tzeng, Cherng-Chyi
European Journal of Medicinal Chemistry, 2005 , vol. 40, # 8 p. 792 - 797
106536-15-6
→
反应条件
57183-50-3
6-甲氧基-2-苯基-4-喹诺酮
反应条件
1: 78 percent / K2CO3 / dimethylformamide / 3 h / 140 °C 2: 82 percent / diphenyl ether / 1 h / 230 - 250 °C 3: 85 percent / NaOH / ethanol / 6 h / Heating View Scheme
参考文献
Zhao, Yue-Ling; Chen, Yeh-Long; Chang, Feng-Shuo; Tzeng, Cherng-Chyi
European Journal of Medicinal Chemistry, 2005 , vol. 40, # 8 p. 792 - 797
106536-15-6
→
反应条件
57183-54-7
反应条件
1.1: 78 percent / K2CO3 / dimethylformamide / 3 h / 140 °C 2.1: diphenyl ether / 0.5 h / 260 - 280 °C 2.2: NaOH / ethanol / 18 h / Heating 2.3: 83 percent / hydrochloric acid / 5 h / Heating 3.1: 95 percent / POCl3 / 1 h / 80 - 90 °C View Scheme
参考文献
Chen, Yeh-Long; Huang, Chao-Jhieh; Huang, Zun-Yuan; Tseng, Chih-Hua; Chang, Feng-Shuo; Yang, Sheng-Huei; Lin, Shinne-Ren; Tzeng, Cherng-Chyi
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 9 p. 3098 - 3105
98-88-4
苯甲酰氯
→
反应条件
106536-15-6
反应条件
Multi-step reaction with 2 steps 1: triethylamine; magnesium chloride / acetonitrile / 0 - 20 °C2: tributyl-amine; trichlorophosphate / Reflux
参考文献
More, Satish S.; Mohan, T. Krishna; Kumar, Y. Sateesh; Kumar, U.K. Syam; Patel, Navin B. Beilstein Journal of Organic Chemistry, 2011 , vol. 7, p. 831 - 838
106536-15-6
+
108-95-2
苯酚
→
反应条件
110375-46-7
反应条件
With potassium carbonate in N,N-dimethyl-formamide T=140°C; 12 h; Heating;
参考文献
Hormi, Osmo E. O.; Moisio, M. Riitta; Sund, B. Christian Journal of Organic Chemistry, 1987 , vol. 52, # 23 p. 5272 - 5274
