Emmerling, Sebastian G. J.; Langer, Laura B. N.; Pihan, Sascha A.; Lellig, Philipp; Gutmann, Jochen S.
Macromolecules, 2010 , vol. 43, # 11 p. 5033 - 5042
in diethyl ether
(Ar); Me3SnLi added dropwise to Me2SiHCl at -70°C; stirred for 2 h at this temperature; warmed overnight to room temperature; volatile condensed at 0.01 Torr/-196°C; fractionated; elem. anal.;
参考文献
Appler, Hubertus; Neumann, Wilhelm P.
Journal of Organometallic Chemistry, 1986 , vol. 314, p. 247 - 260
1: chloromethyl-trimethyl-silane With magnesium in tetrahydrofuran
2: dimethylmono-chlorosilane in tetrahydrofuran
T=20°C;
3: With hydrogenchloride; water in tetrahydrofuran
参考文献
Leatherman, Mark D.; Peng, Wenqing; Policello, George A.; Rajaraman, Suresh K.; Wagner, Roland; Xia, Zijun
Patent: US2007/269467 A1, 2007 ;
Location in patent: Page/Page column 5 ;
