in dichloromethane N2 atmosphere, addn. of soln. of borane to soln. of stannyl compound at -78 to -60°C (2 h), warming to room temp., stirring (room temp., 1 h); spectroscopic yield 100percent, not isolated;
参考文献
European Journal of Inorganic Chemistry, , # 9 p. 1765 - 1780
in dichloromethane N2 atmosphere, addn. of soln. of stannyl compound to soln. of borane at -70 to -40°C (80 min), slow warming to room temp., stirring (roomtemp., 16 h); NMR-monitoring, not isolated;
参考文献
European Journal of Inorganic Chemistry, , # 9 p. 1765 - 1780
