反应条件
in dichloromethane N2 atmosphere, addn. of soln. of stannyl compound to soln. of borane at -65 to -75°C (90 min), slow warming to room temp., stirring (25°C., 12 h); removement of solvent (25°C, 12 Torr) and Me3SnBr (30°C, 1E-2 Torr or 53-55°C, 12 Torr), MeN(BBr(C4H9))2,MeN(SnMe2Br)(BMeBr)/C4H9B(MeB)r ratio 8:2;
参考文献
Diemer, Stefan; Noeth, Heinrich; Storch, Wolfgang
European Journal of Inorganic Chemistry, 1999 , # 9 p. 1765 - 1780
