hydrogenchloride in chloroform 4h boiling, under inflow of gaseous HCl;
参考文献
Zhurnal Obshchei Khimii, , vol. 16, p. 235 - 242
C.A., , p. 90
→
反应条件
hydrogenchloride; ammonia in acetonitrile EtSnMe3 in CH3CN added to Fe(phen)3(ClO4)3 in CH3CN at 22°C under Ar and soln. stirred for 2 h, drop water added and Fe(II) complex filtered, filtrate dried with MgSO4 and treated with anhyd. aq. NH3, Sn product treated with HCl and sublimed;
参考文献
Journal of the American Chemical Society, , vol. 104, # 5 p. 1319 - 1330
iron(III) chloride in tetrachloromethane; toluene T=25°C; 1.5 h;
参考文献
Bulletin de la Societe Chimique de France, , vol. 2, # 1-2 p. 16 - 20
→
反应条件
ammonia in acetonitrile t-BuSnMe3 in CH3CN added to Fe(phen)3(ClO4)3 in CH3CN at 22°C under Ar and soln. stirred for 2 h, drop water added, Fe(II) complex filtered, filtrate dried with MgSO4 and treated with anhyd. aq. NH3, Sn product treated with HCl and sublimed;
参考文献
Journal of the American Chemical Society, , vol. 104, # 5 p. 1319 - 1330
