potassium fluoride in tetrahydrofuran Solid HgCl2 is added to a soln. of the ethene-compd. in THF at room temp. After 20 h stirring KF is added.; After filtn. and removal of the solvent the residue is sublimed at 80°C/10-E2 torr, giving a highly viscous oil; elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 471, # 1-2 p. 39 - 42
triphenylphosphine in ethanol; acetone byproducts: Ni, triphenylphosphonium sulfide; dropwise addn. of an ethanolic soln. of NiCl2*6H2O to a stirred soln. of ((CH3)3Sn)2S and triphenylphosphine in acetone; refluxing;; filtration;;
参考文献
Doklady Chemistry (English Translation), , vol. 286 - 291, p. 305 - 308
Doklady Akademii Nauk SSSR, , vol. 289, p. 644 - 646
potassium fluoride in tetrahydrofuran MeHgCl is added to a soln. of the ethene-compd. in THF at 70°C for 14 d under stirring and under an inert atmosphere. After this KF is added.; After filtn. and removal of the solvent the residue is sublimed at 80°C/10-E2 torr, giving a highly viscous oil; elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 471, # 1-2 p. 39 - 42
potassium fluoride in tetrahydrofuran Solid HgCl2 is added to a soln. of the ethene-compd. in THF at room temp. After 20 h stirring KF is added.; After filtn. and removal of the solvent the residue is sublimed at 80°C/10-E2 torr; elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 471, # 1-2 p. 39 - 42
