反应条件
(Ph3P)2Pd(Ph)(I) in diethyl ether addn. of Me3SnCl in ether to soln. of LiAlH4 in ether (stirring), stirring (20°C, 4 h), addn. of water, addn. of catalyst to intermediate; removal of ether (vac., 1 h), sepn. of Pd-complexes (<20°C, 0.1 Torr), extn. (pentane), drying (over Na2SO4), filtration, redistn.;
参考文献
Bumagin, N. A.; Gulevich, Yu. V.; Beletskaya, I. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, p. 2338 - 2338
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , vol. 31, p. 2639 - 2639
