反应条件
n-butyllithium in tetrahydrofuran; hexane
under Ar; hexane soln. of n-BuLi (1 equiv.) added dropwise over 7 min tosoln. of tetrathiafulvalene in THF at -78°C; stirred (-78.degree .C, 1 h); soln. of Me3SnCl (1.6 equiv.) in THF added at -78°C over 10 min; stirred (-78°C, 1 h); warmed slowly to room temp.; stirred at room temp. for 1 h; diluted by addition of hexane; filtered through Hyflo Super Cel; filtrate concd. in vac.;
参考文献
Iyoda, Masahiko; Hara, Kenji; Ogura, Eiji; Takano, Takahiro; Hasegawa, Masashi; Yoshida, Masato; Kuwatani, Yoshiyuki; Nishikawa, Hiroyuki; Kikuchi, Koichi; Ikemoto, Isao; Mori, Takehiko
Journal of Solid State Chemistry, 2002 , vol. 168, # 2 p. 597 - 607
